Production Cost Report
ICC - Is Bespoken: 0
ICC - Main References: ?
ICC - Issue: D
ICC - Volume: 49
ICC - Report ID: 049-D
ICC - Report Location: United States
ICC - Is Popular: 0
ICC - Is Developed: 1
ICC - Title: Caprolactam from Cyclohexane (Oximation with Hydroxylamine)
ICC - Show Overview: 1
ICC - Report Location ID: 1
ICC - Plant Capacity Unit ID: 14
ICC - Volume Reports List: 049-A,049-B,049-C,049-D,049-E,049-F,049-G,049-H
ICC - Related Reports List: 222-B,222-A,047-A,047-B,070-A,070-B,246-A,246-C
ICC - Report Location Code: USA
ICC - Delivery Times: {"versions":{"1":{"1":{"time":"10","price":0},"2":{"time":"5","price":"599"}},"2":{"1":{"time":"10","price":0},"2":{"time":"5","price":"599"}},"3":{"1":{"time":"12","price":0},"2":{"time":"7","price":"599"}}},"unit":"d"}
ICC - Prices: {"versions":{"1":{"1":"1199","2":"1199","3":"1199"},"2":{"1":"1999","2":"1999","3":"1999"},"3":{"1":"3399","2":"3399","3":"3399"}},"currency":"USD"}
ICC - Plant Capacity Unit Name: kilo metric ton per annum
ICC - Plant Capacity Unit Short Name: kta
ICC - Process Overview Image: //cdn.intratec.us/images/icc/process-overview/049-D.jpg
ICC - Process Overview Text: <h6>Products</h6> <p><b>Caprolactam</b></p>, <p><b>Ammonium Sulfate</b></p> <h6>Raw Materials</h6> <p><b>Hydrogen</b></p>, <p><b>Chemicals</b></p>, <p><b>Ammonia</b></p>, <p><b>Sulfuric Acid</b></p>, <p><b>Cyclohexane</b></p>, <p><b>Oleum</b></p>
ICC - Process Schematic Image: //cdn.intratec.us/images/icc/process-schematics/049-D.jpg
ICC - Process Schematic Text: <p>The process under analysis comprises four major sections: (1) cyclohexanone production; (2) oximation & Beckmann rearrangement; (3) Caprolactam purification; and (4) ammonium sulfate purification.</p><p>Cyclohexanone production. The cyclohexane is converted to a mixture of cyclohexanone and cyclohexanol by liquid-phase air oxidation in the presence of a soluble cobalt catalyst. The cyclohexanol in the mixture is converted to cyclohexanone by vapor-phase dehydrogenation in the presence of a copper-magnesium catalyst. Purified cyclohexanone is obtained after neutralization and distillation steps.</p><p>Oximation & Beckmann rearrangement. Ammonia is oxidized by oxygen in the presence of steam, yielding nitric oxide, which is absorbed in a solution. This nitric oxide is hydrogenated over a palladium catalyst, in the presence of dilute sulfuric acid, producing hydroxylammonium sulfate solution. It reacts with cyclohexanone in stirred reactors in series. The heterogeneous outlet is neutralized with ammonia. Finally, the cyclohexanone oxime is converted to Caprolactam by Beckmann rearrangement, in the presence of oleum.</p><p>Caprolactam purification. The product of rearrangement is subjected to purification steps, involving neutralization, extraction in the presence of toluene and light impurities removal. The raw Caprolactam melt is transformed into crystals that are melted, solidified on cold surface and the flakes produced are packed and sent to storage facilities.</p><p>Ammonium sulfate purification. Ammonium sulfate solution removed in neutralization steps is concentrated by means of evaporation. Then, it is crystallized, centrifuged from mother liquor and dried.</p>
ICC - Short Description: This report presents the economics of Caprolactam production from cyclohexane located in the United States. Initially, cyclohexane is oxidized to a cyclohexanol/cyclohexanone. Then, the cyclohexanol is hydrogenated to cyclohexanone, which is submitted to an oximation reaction with hydroxylamine. Finally, the cyclohexanone oxime produced is converted to Caprolactam by Beckmann rearrangement.
ICC - Main Product: Caprolactam
ICC - Plant Capacity: 180.00
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Caprolactam from Cyclohexane (Oximation with Hydroxylamine)

Caprolactam Production Costs Report | Issue D | Q2 2024

Production Cost Report

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180 kta United States-based plant   |   Q2 2024   |   107 pages   |   Delivered in PDF

This report presents a cost analysis of a 180 kta (kilo metric ton per annum) United States-based plant. You can add a customized cost analysis, assuming another location (country), when ordering a premium edition of this report.

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Production Process Information

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Production Process Information

Process Consumptions

Labor Requirements

Plant Capital Cost Summary

Operating Cost Summary

Production Costs Datasheet

Plant Capital Cost Details

Operating Cost Details

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Plant Capacity Assessment

Process Flow Diagrams

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Content Highlights

Plant Capital Cost Summary

Summary outlining the capital cost required for building the Caprolactam production plant examined

Plant Capital Cost Details

Detailing of fixed capital (ISBL, OSBL & Owner’s Cost), working capital and additional capital requirements

Plant Cost Breakdowns

Breakdown of Caprolactam process unit (ISBL) costs and infrastructure (OSBL) costs; plant cost breakdown per discipline

Operating Costs Summary

Summary presenting the operating variable costs and the total operating cost of the Caprolactam production plant studied

Operating Cost Details

Detailing of utilities costs, operating fixed costs and depreciation

Plant Capacity Assessment

Comparative analysis of capital investment and operating costs for different Caprolactam plant capacities

Production Process Information

Block Flow Diagram, descriptions of process unit (ISBL) and site infrastructure (OSBL)

Process Consumptions

Raw materials and utilities consumption figures, by-products credits, labor requirements

Process Diagrams

Process flow diagrams (PFD), equipment list and industrial site configuration

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This report presents the economics of Caprolactam production from benzene located in the United States. Initially, benzene is hydrogenated to cyclohexane, which is oxidized to cyclohexanone. Then, the cyclohexanone undergoes an oximation reaction with hydroxylamine. Finally, the oxime produced is rearranged to Caprolactam.

Details: 180 kta United States-based plant   |   Q2 2024   |   107 pages   |   Issue A   From $1,499 USD

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Caprolactam Production from Butadiene and Hydrogen Cyanide

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The cost analyses presented in this report target a 180 kta (kilo metric ton per annum per annum) United States-based plant. For those interested in cost analyses considering other plant capacities and/or locations, Intratec offers a customized analysis as an optional feature.

Caprolactam Production from Butadiene, CO, Hydrogen and Ammonia

This report presents the cost associated with a plant located in the United States producing Caprolactam from butadiene, carbon monoxide, hydrogen, and ammonia. The process under analysis involves the following steps: reaction of carbon monoxide with butadiene; hydrocarbonylation; amination and cyclization.

Details: 180 kta United States-based plant   |   Q2 2024   |   107 pages   |   Issue C   From $1,499 USD

The cost analyses presented in this report target a 180 kta (kilo metric ton per annum per annum) United States-based plant. For those interested in cost analyses considering other plant capacities and/or locations, Intratec offers a customized analysis as an optional feature.

Caprolactam from Cyclohexane (Oximation with Hydroxylamine)

This report presents the economics of Caprolactam production from cyclohexane located in the United States. Initially, cyclohexane is oxidized to a cyclohexanol/cyclohexanone. Then, the cyclohexanol is hydrogenated to cyclohexanone, which is submitted to an oximation reaction with hydroxylamine. Finally, the cyclohexanone oxime produced is converted to Caprolactam by Beckmann rearrangement.

Details: 180 kta United States-based plant   |   Q2 2024   |   107 pages   |   Issue D   From $1,199 USD

The cost analyses presented in this report target a 180 kta (kilo metric ton per annum per annum) United States-based plant. For those interested in cost analyses considering other plant capacities and/or locations, Intratec offers a customized analysis as an optional feature.

Caprolactam Production from Phenol

This feasibility study examines the economics of a process producing Caprolactam from phenol located in the United States. Initially, phenol is hydrogenated to form cyclohexanone. The cyclohexanone is then submitted to an oximation reaction with hydroxylamine. Finally, the cyclohexanone oxime produced is converted to caprolactam by Beckmann rearrangement.

Details: 180 kta United States-based plant   |   Q2 2024   |   107 pages   |   Issue E   From $1,199 USD

The cost analyses presented in this report target a 180 kta (kilo metric ton per annum per annum) United States-based plant. For those interested in cost analyses considering other plant capacities and/or locations, Intratec offers a customized analysis as an optional feature.

Caprolactam from Cyclohexane (Photonitrozation Process)

This report concerns the production of Caprolactam from cyclohexane in the United States. This report reviews a cyclohexane photonitrozation process (PNC). Initially, cyclohexane is submitted to PNC with nitrosyl chloride. The oxime produced is then subjected to Beckmann rearrangement and Caprolactam is formed.

Details: 180 kta United States-based plant   |   Q2 2024   |   107 pages   |   Issue F   From $1,499 USD

The cost analyses presented in this report target a 180 kta (kilo metric ton per annum per annum) United States-based plant. For those interested in cost analyses considering other plant capacities and/or locations, Intratec offers a customized analysis as an optional feature.

Caprolactam Production from Toluene

This study reviews the economics of a process for Caprolactam production from toluene. Initially, toluene is oxidized to benzoic acid, which is then hydrogenated to hexahydrobenzoic acid. The hexahydrobenzoic acid is reacted with nitrosyl sulfuric acid and oleum for caprolactam production. The economic analysis performed is based on a plant constructed in the United States.

Details: 180 kta United States-based plant   |   Q2 2024   |   107 pages   |   Issue G   From $1,499 USD

The cost analyses presented in this report target a 180 kta (kilo metric ton per annum per annum) United States-based plant. For those interested in cost analyses considering other plant capacities and/or locations, Intratec offers a customized analysis as an optional feature.

Caprolactam Production from Cyclohexanone

This report presents the economics of Caprolactam production from cyclohexanone in a plant located in the United States. In the process examined, the cyclohexanone feed undergoes an oximation reaction with hydroxilamine. The oxime produced is rearranged to Caprolactam.

Details: 180 kta United States-based plant   |   Q2 2024   |   107 pages   |   Issue H   From $799 USD

The cost analyses presented in this report target a 180 kta (kilo metric ton per annum per annum) United States-based plant. For those interested in cost analyses considering other plant capacities and/or locations, Intratec offers a customized analysis as an optional feature.

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Details: 200 kta United States-based plant   |   Q2 2024   |   107 pages   |   Issue A   From $799 USD

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